Publication Details

Category Text Publication
Reference Category Journals
DOI 10.1016/S0021-9673(97)00337-3
Title (Primary) Application of accelerated solvent extraction followed by gas chromatography, high-performance liquid chromatography and gas chromatography mass spectrometry for the determination of polycyclic aromatic hydrocarbons, chlorinated pesticides and polychlorinated dibenzo-p-dioxins and dibenzofurans in solid wastes
Author Popp, P.; Keil, P.; Möder, M.; Paschke, A.; Thuß, U.
Journal Journal of Chromatography A
Year 1997
Department OEC; ANA
Volume 774
Issue 1-2
Page From 203
Page To 211
Language englisch
Keywords extraction methods; accelerated solvent extraction; environmental analysis; soil
Abstract

Accelerated solvent extraction (ASE) is a new method for the extraction of organic compounds from soils, sludges and other wastes. Due to the elevated temperatures and pressures, the ASE is a time-saving procedure with low consumption of solvents. Applications of this procedure for the determination of chlorinated pesticides in contaminated soils, for the determination of polycyclic aromatic hydrocarbons in heap material, slurry from copper smelting (Theissenschlamm) and soils and for the determination of polychlorinated dibenzo-p-dioxins and dibenzofurans in a fly ash sample are given. Optimization of the procedure relating to extraction time, number of extractions and solvents is described. Comparisons with other extraction methods (Soxhlet extraction and automated Soxhlet extraction) are carried out.

Persistent UFZ Identifier https://www.ufz.de/index.php?en=20939&ufzPublicationIdentifier=9544
Popp, P., Keil, P., Möder, M., Paschke, A., Thuß, U. (1997):
Application of accelerated solvent extraction followed by gas chromatography, high-performance liquid chromatography and gas chromatography mass spectrometry for the determination of polycyclic aromatic hydrocarbons, chlorinated pesticides and polychlorinated dibenzo-p-dioxins and dibenzofurans in solid wastes
J. Chromatogr. A 774 (1-2), 203 - 211