Publication Details

Category Text Publication
Reference Category Journals
DOI 10.1002/anie.200603036
Title (Primary) Acquisition regime for high-resolution heteronuclear 2D NMR spectra
Author Baskyr, I.; Brand, T.; Findeisen, M.; Berger, S.
Source Titel Angewandte Chemie-International Edition
Year 2006
Department TUCHEM
Volume 45
Issue 46
Page From 7821
Page To 7824
Language englisch
Keywords analytical methods; NMR spectroscopy; pulse sequences; structure elucidation
Abstract Double take: In the acquisition regime presented here, 1H,13C HSQC spectra are recorded twice with spectral widths of 5.8 and 6.2 ppm in the indirect dimension. The aliased signals are then unfolded to the full spectral width to yield an HSQC spectrum with 5 Hz per point in the 13C dimension without additional time requirements (see example of strychnine).
Persistent UFZ Identifier https://www.ufz.de/index.php?en=20939&ufzPublicationIdentifier=2475
Baskyr, I., Brand, T., Findeisen, M., Berger, S. (2006):
Acquisition regime for high-resolution heteronuclear 2D NMR spectra
Angew. Chem.-Int. Edit. 45 (46), 7821 - 7824 10.1002/anie.200603036