Details zur Publikation |
| Kategorie | Textpublikation |
| Referenztyp | Zeitschriften |
| DOI | 10.1365/s10337-003-0112-9 |
| Volltext | Shareable Link |
| Titel (primär) | A new method for the sensitive analysis of ochratoxin A in house dust |
| Autor | Köller, G.; Rolle-Kampczyk, U.; Popp, P.; Herbarth, O. |
| Quelle | Chromatographia |
| Erscheinungsjahr | 2003 |
| Department | ANA; EXPOEPID |
| Band/Volume | 58 |
| Heft | 11/12 |
| Seite von | 763 |
| Seite bis | 767 |
| Sprache | englisch |
| Keywords | Capillary electrophoresis; House dust; Ochratoxin A; Sample stacking |
| Abstract | A sensitive method for the analysis of Ochratoxin A (OA) in house dust is described using capillary zone electrophoresis coupled to laser-induced fluorescence. The methods sensitivity makes it suitable for determining OA from just 500 mg house dust. The house dust is extracted with acetonitrile. The extract is purified in a two-step sample clean-up. The first step is liquid-liquid extraction with dichloromethane followed by normal-phase solid phase extraction. The estimated recovery of OA exceeds 82%. Capillary electrophoresis with a developed sample stacking procedure with reversed polarity provides a low limit of detection of 0.2 ng g-1 in house dust. The buffer system and the injected volume are optimized. To enhance reproducibility and ensure proper peak identification, an internal standard was added to the method. |
| dauerhafte UFZ-Verlinkung | https://www.ufz.de/index.php?en=20939&ufzPublicationIdentifier=4993 |
| Köller, G., Rolle-Kampczyk, U., Popp, P., Herbarth, O. (2003): A new method for the sensitive analysis of ochratoxin A in house dust Chromatographia 58 (11/12), 763 - 767 10.1365/s10337-003-0112-9 |
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