Details zur Publikation

Referenztyp Zeitschriften
DOI / URL Link
Titel (primär) Acquisition regime for high-resolution heteronuclear 2D NMR spectra
Autor Baskyr, I.; Brand, T.; Findeisen, M.; Berger, S.;
Journal / Serie Angewandte Chemie-International Edition
Erscheinungsjahr 2006
Department TUCHEM;
Band/Volume 45
Heft 46
Sprache englisch;
Keywords analytical methods; NMR spectroscopy; pulse sequences; structure elucidation
Abstract Double take: In the acquisition regime presented here, 1H,13C HSQC spectra are recorded twice with spectral widths of 5.8 and 6.2 ppm in the indirect dimension. The aliased signals are then unfolded to the full spectral width to yield an HSQC spectrum with 5 Hz per point in the 13C dimension without additional time requirements (see example of strychnine).
ID 2475
dauerhafte UFZ-Verlinkung https://www.ufz.de/index.php?en=20939&ufzPublicationIdentifier=2475
Baskyr, I., Brand, T., Findeisen, M., Berger, S. (2006):
Acquisition regime for high-resolution heteronuclear 2D NMR spectra
Angew. Chem.-Int. Edit. 45 (46), 7821 - 7824