Details zur Publikation |
| Kategorie | Textpublikation |
| Referenztyp | Zeitschriften |
| DOI | 10.1002/anie.200603036 |
| Titel (primär) | Acquisition regime for high-resolution heteronuclear 2D NMR spectra |
| Autor | Baskyr, I.; Brand, T.; Findeisen, M.; Berger, S. |
| Quelle | Angewandte Chemie-International Edition |
| Erscheinungsjahr | 2006 |
| Department | TUCHEM |
| Band/Volume | 45 |
| Heft | 46 |
| Seite von | 7821 |
| Seite bis | 7824 |
| Sprache | englisch |
| Keywords | analytical methods; NMR spectroscopy; pulse sequences; structure elucidation |
| Abstract | Double take: In the acquisition regime presented here, 1H,13C HSQC spectra are recorded twice with spectral widths of 5.8 and 6.2 ppm in the indirect dimension. The aliased signals are then unfolded to the full spectral width to yield an HSQC spectrum with 5 Hz per point in the 13C dimension without additional time requirements (see example of strychnine). |
| dauerhafte UFZ-Verlinkung | https://www.ufz.de/index.php?en=20939&ufzPublicationIdentifier=2475 |
| Baskyr, I., Brand, T., Findeisen, M., Berger, S. (2006): Acquisition regime for high-resolution heteronuclear 2D NMR spectra Angew. Chem.-Int. Edit. 45 (46), 7821 - 7824 10.1002/anie.200603036 |
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